N-linked oligosaccharides of cobra venom factor contain novel α(1-3)galactosylated Lex structures

نویسندگان

  • D. Channe Gowda
  • John Glushka
  • Herman van Halbeek
  • Rao N. Thotakura
  • Reinhard Bredehorst
  • Vincent T. Lombardi
چکیده

Cobra venom factor (CVF), a nontoxic, complementactivating glycoprotein in cobra venom, is a functional analog of mammalian complement component C3b. The carbohydrate moiety of CVF consists exclusively of N-linked oligosaccharides with terminal α1-3-linked galactosyl residues, which are antigenic in human. CVF has potential for several medical applications, including targeted cell killing and complement depletion. Here, we report a detailed structural analysis of the oligosaccharides of CVF. The structures of the oligosaccharides were determined by lectin affinity chromatography, antibody affinity blotting, compositional and methylation analyses, and high-resolution 1H-NMR spectroscopy. Approximately 80% of the oligosaccharides are diantennary complex-type, ∼12% are triand tetra-antennary complex-type, and ∼8% are oligomannose type structures. The majority of the complex-type oligosaccharides terminate in Galα1-3Galβ1-4(Fucα1-3)GlcNAcβ1, a unique carbohydrate structural feature abundantly present in the glycoproteins of cobra venom.

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تاریخ انتشار 2001